Information card for entry 7133334

Structure parameters

• Formula: C24 H32 B Cr N4 Na O8
• Calculated formula: C24 H32 B Cr N4 Na O8
• Title of publication: The tetracyanoborate anion as a building block for the heterocubane cluster cage [Cr₄{B(CN)₄}₄]⁴.
• Authors of publication: Luff, Martin S.; Bertermann, Rüdiger; Finze, Maik; Radius, Udo
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 65
• Pages of publication: 8621 - 8624
• a: 9.8572 ± 0.0004 Å
• b: 12.1418 ± 0.0005 Å
• c: 12.9109 ± 0.0005 Å
• α: 100.325 ± 0.003°
• β: 96.817 ± 0.003°
• γ: 95.944 ± 0.003°
• Cell volume: 1497.09 ± 0.11 ų
• Cell temperature: 568 ± 2 K
• Ambient diffraction temperature: 568 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0809
• Residual factor for significantly intense reflections: 0.0758
• Weighted residual factors for significantly intense reflections: 0.2178
• Weighted residual factors for all reflections included in the refinement: 0.2232
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No