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Information card for entry 7133413
Preview
Coordinates | 7133413.cif |
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Original paper (by DOI) | HTML |
Formula | C20 H13 Br O2 |
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Calculated formula | C20 H13 Br O2 |
Title of publication | Catalytic asymmetric construction of bridged bicyclo[<i>m</i>.3.1] rings using an intramolecular Diels-Alder reaction. |
Authors of publication | Li, Kai; Zhao, Zhengxing; Qin, Wenling; Liu, Yidong; Yan, Hailong |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2024 |
Journal volume | 60 |
Journal issue | 71 |
Pages of publication | 9570 - 9573 |
a | 8.0085 ± 0.0003 Å |
b | 8.9848 ± 0.0006 Å |
c | 21.0224 ± 0.0011 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1512.66 ± 0.14 Å3 |
Cell temperature | 295 ± 2 K |
Ambient diffraction temperature | 295 ± 2 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0644 |
Residual factor for significantly intense reflections | 0.0439 |
Weighted residual factors for significantly intense reflections | 0.0728 |
Weighted residual factors for all reflections included in the refinement | 0.0823 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7133413.html
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