Information card for entry 7133432
| Formula |
C18 H14 F N O2 |
| Calculated formula |
C18 H14 F N O2 |
| Title of publication |
Palladium-catalyzed 1,1-aminoxylation of 3-butenoic acid with 2-alkynylanilines. |
| Authors of publication |
Zhang, Jinhui; Mao, Lihua; Liu, Chao; Tan, Xiangwen; Wu, Jiahao; Wei, Xuefeng; Wu, Wanqing; Jiang, Huanfeng |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2024 |
| Journal volume |
60 |
| Journal issue |
70 |
| Pages of publication |
9404 - 9407 |
| a |
9.277 ± 0.0006 Å |
| b |
9.5602 ± 0.0006 Å |
| c |
9.7665 ± 0.0006 Å |
| α |
104.289 ± 0.002° |
| β |
110.312 ± 0.002° |
| γ |
107.388 ± 0.002° |
| Cell volume |
713.26 ± 0.08 Å3 |
| Cell temperature |
170 K |
| Ambient diffraction temperature |
170 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.1178 |
| Residual factor for significantly intense reflections |
0.0529 |
| Weighted residual factors for significantly intense reflections |
0.1009 |
| Weighted residual factors for all reflections included in the refinement |
0.1309 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.05 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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https://www.crystallography.net/7133432.html
