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Information card for entry 7133438
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Coordinates | 7133438.cif |
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Original paper (by DOI) | HTML |
Formula | C18 H15 N O3 |
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Calculated formula | C18 H15 N O3 |
Title of publication | Transition-metal free, radical oxidation of 1,6-enyne cyclopropanation: synthesis of aza-bicyclo[4.1.0]heptane derivatives. |
Authors of publication | Meena, Shivam A.; Thakur, Deepika; Nandy, Abhijit; Ranjan, Rahul; Rai, Anubhav; Banerjee, Shibdas; Verma, Akhilesh K. |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2024 |
Journal volume | 60 |
Journal issue | 69 |
Pages of publication | 9230 - 9233 |
a | 10.6199 ± 0.0004 Å |
b | 10.8504 ± 0.0005 Å |
c | 15.1555 ± 0.0006 Å |
α | 103.773 ± 0.004° |
β | 97.032 ± 0.003° |
γ | 114.529 ± 0.004° |
Cell volume | 1493.92 ± 0.13 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1049 |
Residual factor for significantly intense reflections | 0.0652 |
Weighted residual factors for significantly intense reflections | 0.1858 |
Weighted residual factors for all reflections included in the refinement | 0.2094 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.07 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7133438.html
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