Information card for entry 7133494

Structure parameters

• Formula: C28 H36 F2 N2
• Calculated formula: C28 H36 F2 N2
• Title of publication: Solid-state [2+2] photodimerization of eniminium salts: stereoselective syntheses of 1,3-diacetylcyclobutanes.
• Authors of publication: Yamada, Shinji; Honda, Yuka
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 72
• Pages of publication: 9821 - 9824
• a: 9.36553 ± 0.00017 Å
• b: 10.40596 ± 0.00019 Å
• c: 12.2778 ± 0.0002 Å
• α: 90°
• β: 99.9106 ± 0.0011°
• γ: 90°
• Cell volume: 1178.71 ± 0.04 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0437
• Residual factor for significantly intense reflections: 0.0355
• Weighted residual factors for significantly intense reflections: 0.0926
• Weighted residual factors for all reflections included in the refinement: 0.1017
• Goodness-of-fit parameter for all reflections included in the refinement: 1.121
• Diffraction radiation wavelength: 1.54187 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No