Crystallography Open Database

Information card for entry 7133523

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Coordinates	7133523.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H48 Cl4 N3 P Pd Si2
Calculated formula	C37 H48 Cl4 N3 P Pd Si2
Title of publication	A hybrid silylene-Pd catalyst: efficient C-N cross-coupling of sterically bulky amines and chiral amines.
Authors of publication	Kaulage, Sandeep H.; Parvin, Nasrina; Khopade, Kishor V.; Khan, Shabana
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	73
Pages of publication	9958 - 9961
a	25.422 ± 0.004 Å
b	11.0674 ± 0.0013 Å
c	33.751 ± 0.004 Å
α	90°
β	109.835 ± 0.006°
γ	90°
Cell volume	8933 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1432
Residual factor for significantly intense reflections	0.0738
Weighted residual factors for significantly intense reflections	0.1011
Weighted residual factors for all reflections included in the refinement	0.1192
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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