Information card for entry 7133586

Structure parameters

• Chemical name: (Î1/4-chloro)-hexakis(3,5-di-t-butylphenyl)-difluoro-di-bismuth tetrakis(3,5-bis(trifluoromethyl)phenyl)borate
• Formula: C116 H138 B Bi2 Cl3 F24
• Calculated formula: C116 H138 B Bi2 Cl3 F24
• Title of publication: Synthesis and characterization of chlorotriarylbismuthonium salts.
• Authors of publication: Kuziola, Jennifer; Nöthling, Nils; Leutzsch, Markus; Cornella, Josep
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 76
• Pages of publication: 10532 - 10535
• a: 34.1234 ± 0.0013 Å
• b: 18.2693 ± 0.0007 Å
• c: 19.4972 ± 0.0008 Å
• α: 90°
• β: 108.812 ± 0.002°
• γ: 90°
• Cell volume: 11505.5 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0394
• Residual factor for significantly intense reflections: 0.0301
• Weighted residual factors for significantly intense reflections: 0.0739
• Weighted residual factors for all reflections included in the refinement: 0.0796
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No