Information card for entry 7133662

Structure parameters

• Formula: C64 H50 Cl4 P2 Re
• Calculated formula: C64 H50 Cl4 P2 Re
• Title of publication: Oxidation-induced coupling reactions of bi(metallacycloprop-1-ene) complexes.
• Authors of publication: Tsang, Long Yiu; Kong, Lam Cheung; Sung, Herman H. Y.; Williams, Ian D.; Jia, Guochen
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 78
• Pages of publication: 10946 - 10949
• a: 15.5823 ± 0.0003 Å
• b: 22.9599 ± 0.0003 Å
• c: 18.0278 ± 0.0003 Å
• α: 90°
• β: 107.943 ± 0.0017°
• γ: 90°
• Cell volume: 6136.06 ± 0.19 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0648
• Residual factor for significantly intense reflections: 0.0443
• Weighted residual factors for significantly intense reflections: 0.1084
• Weighted residual factors for all reflections included in the refinement: 0.1167
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No