Crystallography Open Database

Information card for entry 7133665

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Coordinates	7133665.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H30 N O6
Calculated formula	C28 H30 N O6
Title of publication	Phosphine-catalyzed enantioselective and diastereodivergent [3+2] cyclization for the construction of oxetane dispirooxindole skeletons.
Authors of publication	Han, Xiao; Hou, Jie; Zhang, Haiyan; Wang, Zhen; Yao, Weijun
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	77
Pages of publication	10736 - 10739
a	7.8531 ± 0.0005 Å
b	8.9782 ± 0.0006 Å
c	35.617 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	2511.2 ± 0.3 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170 ± 2 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0883
Residual factor for significantly intense reflections	0.0852
Weighted residual factors for significantly intense reflections	0.2854
Weighted residual factors for all reflections included in the refinement	0.2937
Goodness-of-fit parameter for all reflections included in the refinement	1.188
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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