Information card for entry 7133696

Structure parameters

• Formula: C61 H97 N2 O Si2 Yb
• Calculated formula: C61 H97 N2 O Si2 Yb
• Title of publication: CO reduction by calcium and ytterbium hydride complexes with a bulky monodentate carbazolyl ligand.
• Authors of publication: Hinz, Alexander; Winkler, Lucas; Sun, Xiaofei
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 80
• Pages of publication: 11291 - 11294
• a: 11.7801 ± 0.0006 Å
• b: 14.1233 ± 0.0008 Å
• c: 18.7536 ± 0.001 Å
• α: 92.001 ± 0.004°
• β: 106.563 ± 0.004°
• γ: 92.221 ± 0.004°
• Cell volume: 2985 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1011
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.0985
• Weighted residual factors for all reflections included in the refinement: 0.1095
• Goodness-of-fit parameter for all reflections included in the refinement: 0.831
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.34143 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No