Information card for entry 7133717

Structure parameters

• Formula: C27 H27 N O
• Calculated formula: C27 H27 N O
• Title of publication: Palladium/norbornene-catalyzed C-H/N-H cycloaddition of carbazoles with 2-halobenzoic acid derivatives
• Authors of publication: Liu, Shilei; Nan, Jiang; An, Nan; Cao, Rui; Zhu, Lanxin; Yan, Qiang; Zhang, Hanqing; Liang, Chengyuan
• Journal of publication: Chemical Communications
• Year of publication: 2024
• a: 7.057 ± 0.003 Å
• b: 12.282 ± 0.004 Å
• c: 13.493 ± 0.005 Å
• α: 76.338 ± 0.013°
• β: 79.786 ± 0.014°
• γ: 78.458 ± 0.014°
• Cell volume: 1103 ± 0.7 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1377
• Residual factor for significantly intense reflections: 0.0746
• Weighted residual factors for significantly intense reflections: 0.2036
• Weighted residual factors for all reflections included in the refinement: 0.2676
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No