Information card for entry 7133999

Structure parameters

• Formula: C36 H28 F6 N2 O2
• Calculated formula: C36 H28 F6 N2 O2
• Title of publication: Ring Expansion of 3-Hydroxyoxindoles to 4-Quinolones via Palladium-Catalyzed C–C(acyl) Bond Cleavage and Subsequent Camps Cyclization
• Authors of publication: Huang, Zhi-Cong; Ruan, Zhi-Ling; Dai, Hui-Xiong; Xu, Hui
• Journal of publication: Chemical Communications
• Year of publication: 2024
• a: 25.784 ± 0.002 Å
• b: 6.9333 ± 0.0006 Å
• c: 16.7815 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3000 ± 0.5 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.1363
• Residual factor for significantly intense reflections: 0.0628
• Weighted residual factors for significantly intense reflections: 0.1427
• Weighted residual factors for all reflections included in the refinement: 0.1911
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No