Information card for entry 7134387

Structure parameters

• Formula: C24 H26 N2 O
• Calculated formula: C24 H26 N2 O
• Title of publication: Palladium-catalysed alleneamination of γ,δ-unsaturated hydrazones with propargylic acetates: access to tetrahydropyridazines bearing allenes
• Authors of publication: Wu, Shuaijie; Xu, Shiji; He, Yanru; Sun, Jing; Jiang, Wei; Yan, Chao-Guo; Hu, Weiming; Wang, Lei
• Journal of publication: Chemical Communications
• Year of publication: 2025
• Journal volume: 61
• Journal issue: 36
• Pages of publication: 6647 - 6650
• a: 7.1976 ± 0.0004 Å
• b: 23.2687 ± 0.0013 Å
• c: 24.5001 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4103.2 ± 0.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.146
• Residual factor for significantly intense reflections: 0.0585
• Weighted residual factors for significantly intense reflections: 0.0885
• Weighted residual factors for all reflections included in the refinement: 0.1091
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No