Information card for entry 7150168
Formula
C20 H18 O4
Calculated formula
C20 H18 O4
SMILES
O1C(=O)[C@]2(C[C@@H]([C@H]2c2c1cccc2)c1ccccc1)C(=O)OCC.O1C(=O)[C@@]2(C[C@H]([C@@H]2c2c1cccc2)c1ccccc1)C(=O)OCC
Title of publication
Novel stereoconvergent transformation of 1,2a-disubstituted 1,2,2a,8b-tetrahydro-3H-benzo[b]cyclobuta[d]pyran-3-ones to 1,3-disubstituted 1,2,4a,9b-tetrahydrodibenzofuran-4-ols and its application to the second-generation synthesis of (+/-)-linderol A.
Authors of publication
Yamashita, Masayuki; Inaba, Tomoki; Nagahama, Masaki; Shimizu, Takashi; Kosaka, Sachiko; Kawasaki, Ikuo; Ohta, Shunsaku
Journal of publication
Organic & biomolecular chemistry
Year of publication
2005
Journal volume
3
Journal issue
12
Pages of publication
2296 - 2304
a
8.471 ± 0.001 Å
b
11.811 ± 0.002 Å
c
16.531 ± 0.003 Å
α
90°
β
90°
γ
90°
Cell volume
1653.9 ± 0.5 Å3
Cell temperature
296.2 K
Number of distinct elements
3
Space group number
33
Hermann-Mauguin space group symbol
P n a 21
Hall space group symbol
P 2c -2n
Residual factor for significantly intense reflections
0.0606
Weighted residual factors for all reflections included in the refinement
0.1894
Goodness-of-fit parameter for all reflections included in the refinement
1.744
Diffraction radiation wavelength
1.5418 Å
Diffraction radiation type
CuKα
Has coordinates
Yes
Has disorder
No
Has Fobs
No
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The link is:
https://www.crystallography.net/7150168.html