Information card for entry 7150270

Structure parameters

• Formula: C23 H32 O2
• Calculated formula: C23 H32 O2
• Title of publication: A new and efficient method for o-quinone methide intermediate generation: application to the biomimetic synthesis of the benzopyran derived natural products (+/-)-lucidene and (+/-)-alboatrin.
• Authors of publication: Rodriguez, Raphaël; Moses, John E.; Adlington, Robert M.; Baldwin, Jack E.
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2005
• Journal volume: 3
• Journal issue: 19
• Pages of publication: 3488 - 3495
• a: 19.4765 ± 0.0003 Å
• b: 9.6966 ± 0.0002 Å
• c: 21.0587 ± 0.0004 Å
• α: 90°
• β: 94.5151 ± 0.0008°
• γ: 90°
• Cell volume: 3964.72 ± 0.13 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0853
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for all reflections: 0.0695
• Weighted residual factors for significantly intense reflections: 0.0524
• Weighted residual factors for all reflections included in the refinement: 0.0524
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No