Information card for entry 7150444

Structure parameters

• Formula: C24 H38 N2 O3 S Si2
• Calculated formula: C24 H38 N2 O3 S Si2
• Title of publication: First asymmetric synthesis of a differentially silyl-protected tris(alkynyl)methyl methyl ether.
• Authors of publication: Convertino, Vito; Manini, Peter; Schweizer, W. Bernd; Diederich, François
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2006
• Journal volume: 4
• Journal issue: 7
• Pages of publication: 1206 - 1208
• a: 11.2537 ± 0.0002 Å
• b: 13.9426 ± 0.0002 Å
• c: 28.9064 ± 0.0005 Å
• α: 83.0511 ± 0.0006°
• β: 88.3274 ± 0.0005°
• γ: 82.8675 ± 0.0009°
• Cell volume: 4466.96 ± 0.13 ų
• Cell temperature: 172 K
• Number of distinct elements: 6
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0827
• Residual factor for significantly intense reflections: 0.0724
• Weighted residual factors for significantly intense reflections: 0.1961
• Weighted residual factors for all reflections included in the refinement: 0.2102
• Goodness-of-fit parameter for all reflections included in the refinement: 1.625
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No