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Information card for entry 7150855
Preview
Coordinates | 7150855.cif |
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Original paper (by DOI) | HTML |
Common name | 3,3-Spiro-bis((5-(E)-4-ethylbenzylidene)piperidine-2,6-dione) |
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Chemical name | 3,3-Spiro-bis[{5-(E)-4-ethylbenzylidene}piperidine-2,6-dione] |
Formula | C27 H26 N2 O4 |
Calculated formula | C27 H26 N2 O4 |
SMILES | O=C1NC(=O)C(=C\c2ccc(cc2)CC)\CC21C/C(=C\c1ccc(cc1)CC)C(=O)NC2=O |
Title of publication | Simple and facile synthesis of tetralone-spiro-glutarimides and spiro-bisglutarimides from Baylis‒Hillman acetates |
Authors of publication | Basavaiah, Deevi; Reddy, Raju Jannapu |
Journal of publication | Organic & Biomolecular Chemistry |
Year of publication | 2008 |
Journal volume | 6 |
Journal issue | 6 |
Pages of publication | 1034 - 1039 |
a | 10.0689 ± 0.0007 Å |
b | 10.7855 ± 0.0008 Å |
c | 12.4469 ± 0.0009 Å |
α | 101.142 ± 0.001° |
β | 108.914 ± 0.001° |
γ | 105.628 ± 0.001° |
Cell volume | 1171.6 ± 0.15 Å3 |
Cell temperature | 298 K |
Ambient diffraction temperature | 298 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0803 |
Residual factor for significantly intense reflections | 0.0617 |
Weighted residual factors for significantly intense reflections | 0.1824 |
Weighted residual factors for all reflections included in the refinement | 0.1963 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.07 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7150855.html
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