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Information card for entry 7151029
Preview
Coordinates | 7151029.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C45 H40 Ge O2 |
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Calculated formula | C45 H40 Ge O2 |
SMILES | [Ge]1(O[C@@]2(O[C@@]2(C21c1ccccc1c1ccccc21)c1ccccc1)c1ccccc1)(c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C.[Ge]1(O[C@]2(O[C@]2(C21c1ccccc1c1ccccc21)c1ccccc1)c1ccccc1)(c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C |
Title of publication | An unexpected epoxidation of benzil derivatives in their reaction with a germene |
Authors of publication | El Kettani, Sakina Ech-Cherif; Lazraq, Mohamed; Ouhsaine, Fatima; Gornitzka, Heinz; Ranaivonjatovo, Henri; Escudié, Jean |
Journal of publication | Organic & Biomolecular Chemistry |
Year of publication | 2008 |
Journal volume | 6 |
Journal issue | 21 |
Pages of publication | 4064 - 4066 |
a | 10.828 ± 0.004 Å |
b | 11.7 ± 0.004 Å |
c | 15.348 ± 0.005 Å |
α | 75.228 ± 0.007° |
β | 74.785 ± 0.008° |
γ | 73.428 ± 0.007° |
Cell volume | 1763.9 ± 1.1 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.117 |
Residual factor for significantly intense reflections | 0.0558 |
Weighted residual factors for significantly intense reflections | 0.093 |
Weighted residual factors for all reflections included in the refinement | 0.1095 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.903 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7151029.html
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Users of the data should acknowledge the original authors of the
structural data.