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Information card for entry 7151281
Preview
Coordinates | 7151281.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | 7,8-dihydro-10-(3,4,5-trimethoxyphenyl)-7,7-dimethyl-5-p-tolyl- 5H-indeno[1,2-b]quinoline-9,11(6H,10H)-dione |
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Formula | C34 H34 N O5.5 |
Calculated formula | C34 H34 N O5.5 |
Title of publication | An efficient one-pot, three-component synthesis of indeno[1,2-b]quinoline-9,11(6H,10H)-dione, acridine-1,8(2H,5H)-dione and quinoline-3-carbonitrile derivatives from enaminones. |
Authors of publication | Tu, Shu-Jiang; Jiang, Bo; Jia, Run-Hong; Zhang, Jun-Yong; Zhang, Yan; Yao, Chang-Sheng; Shi, Feng |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2006 |
Journal volume | 4 |
Journal issue | 19 |
Pages of publication | 3664 - 3668 |
a | 25.094 ± 0.006 Å |
b | 12.755 ± 0.003 Å |
c | 19.891 ± 0.005 Å |
α | 90° |
β | 103.926 ± 0.004° |
γ | 90° |
Cell volume | 6179 ± 3 Å3 |
Cell temperature | 298 ± 2 K |
Ambient diffraction temperature | 298 ± 2 K |
Number of distinct elements | 4 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.1921 |
Residual factor for significantly intense reflections | 0.0731 |
Weighted residual factors for significantly intense reflections | 0.1771 |
Weighted residual factors for all reflections included in the refinement | 0.2391 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.998 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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