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Information card for entry 7151331
Preview
Coordinates | 7151331.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C50 H40 Br F3 O2 P2 Pd S |
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Calculated formula | C50 H40 Br F3 O2 P2 Pd S |
Title of publication | Insights into the mechanism of the site-selective sequential palladium-catalyzed cross-coupling reactions of dibromothiophenes/dibromothiazoles and arylboronic acids. Synthesis of PPARbeta/delta agonists. |
Authors of publication | Pereira, Raquel; Furst, Audrey; Iglesias, Beatriz; Germain, Pierre; Gronemeyer, Hinrich; de Lera, Angel R. |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2006 |
Journal volume | 4 |
Journal issue | 24 |
Pages of publication | 4514 - 4525 |
a | 21.459 ± 0.003 Å |
b | 11.2009 ± 0.0016 Å |
c | 22.854 ± 0.003 Å |
α | 90° |
β | 102.583 ± 0.004° |
γ | 90° |
Cell volume | 5361.3 ± 1.3 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1949 |
Residual factor for significantly intense reflections | 0.094 |
Weighted residual factors for significantly intense reflections | 0.2117 |
Weighted residual factors for all reflections included in the refinement | 0.2483 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.986 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7151331.html
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