Information card for entry 7151350

Structure parameters

• Common name: 6c in paper?
• Formula: C27 H30 N2 O3
• Calculated formula: C27 H30 N2 O3
• Title of publication: A diversity oriented four-component approach to tetrahydro-beta-carbolines initiated by Sonogashira coupling.
• Authors of publication: Karpov, Alexei S.; Rominger, Frank; Müller, Thomas J J
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2005
• Journal volume: 3
• Journal issue: 24
• Pages of publication: 4382 - 4391
• a: 15.6913 ± 0.0001 Å
• b: 16.5338 ± 0.0002 Å
• c: 18.142 ± 0.0002 Å
• α: 90°
• β: 99.574 ± 0.001°
• γ: 90°
• Cell volume: 4641.15 ± 0.08 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1037
• Residual factor for significantly intense reflections: 0.0495
• Weighted residual factors for significantly intense reflections: 0.1203
• Weighted residual factors for all reflections included in the refinement: 0.1477
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No