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Information card for entry 7151417
Preview
Coordinates | 7151417.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H34 O3 Si |
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Calculated formula | C27 H34 O3 Si |
SMILES | [Si](OC1=C[C@H]2[C@@]34[C@@](C1)(CC(=C[C@@H]3CC2)C)C(=O)c1c(C4=O)cccc1)(C)(C)C(C)(C)C.[Si](OC1=C[C@@H]2[C@]34[C@](C1)(CC(=C[C@H]3CC2)C)C(=O)c1c(C4=O)cccc1)(C)(C)C(C)(C)C |
Title of publication | An enantioselective double Diels?Alder approach to the tetracyclic framework of colombiasin AElectronic supplementary information (ESI) available: Detailed procedures for the preparation of all compounds and their spectral data. See http://www.rsc.org/suppdata/ob/b3/b302522e/ |
Authors of publication | Chaplin, Jason H.; Edwards, Alison J.; Flynn, Bernard L. |
Journal of publication | Organic & Biomolecular Chemistry |
Year of publication | 2003 |
Journal volume | 1 |
Journal issue | 11 |
Pages of publication | 1842 |
a | 12.9389 ± 0.0002 Å |
b | 11.7515 ± 0.0003 Å |
c | 16.957 ± 0.0004 Å |
α | 90° |
β | 111.055 ± 0.0008° |
γ | 90° |
Cell volume | 2406.2 ± 0.09 Å3 |
Cell temperature | 200 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/a 1 |
Hall space group symbol | -P 2yab |
Residual factor for significantly intense reflections | 0.0349 |
Weighted residual factors for all reflections included in the refinement | 0.0409 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.0528 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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