Information card for entry 7151544

Structure parameters

• Formula: C19 H24 N2 O9 S
• Calculated formula: C19 H24 N2 O9 S
• SMILES: C(=N\NS(=O)(=O)c1ccc(cc1)C)/[C@@H]1[C@H]([C@@H]([C@@H](CO1)OC(=O)C)OC(=O)C)OC(=O)C
• Title of publication: C-Glycosylmethylene carbenes: synthesis of anhydro-aldose tosylhydrazones as precursors; generation and a new synthetic route to exo-glycals
• Authors of publication: Marietta Tóth; Katalin E. Kövér; Attila Bényei; László Somsák
• Journal of publication: Org. Biomol. Chem.
• Year of publication: 2003
• Journal volume: 1
• Journal issue: 22
• Pages of publication: 4039 - 4046
• a: 9.939 ± 0.007 Å
• b: 12.907 ± 0.005 Å
• c: 20.16 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2586 ± 2 ų
• Cell temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for significantly intense reflections: 0.0533
• Weighted residual factors for all reflections included in the refinement: 0.1828
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No