Pyrrolyl-, 2-(2-thienyl)pyrrolyl- and 2,5-bis(2-thienyl)pyrrolyl-nucleosides: synthesis, molecular and electronic structure, and redox behaviour of C5-thymidine derivatives.
Authors of publication
Galindo, Miguel A.; Hannant, Jennifer; Harrington, Ross W.; Clegg, William; Horrocks, Benjamin R.; Pike, Andrew R.; Houlton, Andrew
Journal of publication
Organic & biomolecular chemistry
Year of publication
2011
Journal volume
9
Journal issue
5
Pages of publication
1555 - 1564
a
10.158 ± 0.0006 Å
b
5.7057 ± 0.0003 Å
c
11.3236 ± 0.0007 Å
α
90°
β
111.933 ± 0.007°
γ
90°
Cell volume
608.8 ± 0.07 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.039
Residual factor for significantly intense reflections
0.0285
Weighted residual factors for significantly intense reflections
0.0699
Weighted residual factors for all reflections included in the refinement
0.0723
Goodness-of-fit parameter for all reflections included in the refinement
