Information card for entry 7151653

Structure parameters

• Formula: C53 H45 N2 O11 Tb Zn
• Calculated formula: C53 H45 N2 O11 Tb Zn
• Title of publication: A novel synthesis of oxazolidine-2,4-diones via an efficient fixation of CO2 with 3-aryl-2-alkynamides.
• Authors of publication: Chen, Guofei; Fu, Chunling; Ma, Shengming
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2011
• Journal volume: 9
• Journal issue: 1
• Pages of publication: 105 - 110
• a: 13.028 ± 0.003 Å
• b: 13.163 ± 0.003 Å
• c: 15.397 ± 0.003 Å
• α: 75.58 ± 0.03°
• β: 82.38 ± 0.03°
• γ: 83.32 ± 0.03°
• Cell volume: 2525.1 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0586
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.0955
• Weighted residual factors for all reflections included in the refinement: 0.0992
• Goodness-of-fit parameter for all reflections included in the refinement: 0.986
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No