Information card for entry 7152223

Structure parameters

• Formula: C24 H23 N Si
• Calculated formula: C24 H23 N Si
• SMILES: C[Si]1(C)Cc2ccccc2c2c1n(c1c2cccc1)c1ccc(cc1)C
• Title of publication: Palladium-catalyzed silyl C(sp(3))-H bond activation.
• Authors of publication: Liang, Yun; Geng, Weizhi; Wei, Junnian; Ouyang, Kunbing; Xi, Zhenfeng
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2012
• Journal volume: 10
• Journal issue: 8
• Pages of publication: 1537 - 1542
• a: 9.3619 ± 0.0019 Å
• b: 10.083 ± 0.002 Å
• c: 10.655 ± 0.002 Å
• α: 87.11 ± 0.03°
• β: 82.02 ± 0.03°
• γ: 88.24 ± 0.03°
• Cell volume: 994.5 ± 0.3 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1855
• Residual factor for significantly intense reflections: 0.0664
• Weighted residual factors for significantly intense reflections: 0.1178
• Weighted residual factors for all reflections included in the refinement: 0.1398
• Goodness-of-fit parameter for all reflections included in the refinement: 0.996
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No