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Information card for entry 7152223
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Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 7152223.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H23 N Si |
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Calculated formula | C24 H23 N Si |
SMILES | C[Si]1(C)Cc2ccccc2c2c1n(c1c2cccc1)c1ccc(cc1)C |
Title of publication | Palladium-catalyzed silyl C(sp(3))-H bond activation. |
Authors of publication | Liang, Yun; Geng, Weizhi; Wei, Junnian; Ouyang, Kunbing; Xi, Zhenfeng |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2012 |
Journal volume | 10 |
Journal issue | 8 |
Pages of publication | 1537 - 1542 |
a | 9.3619 ± 0.0019 Å |
b | 10.083 ± 0.002 Å |
c | 10.655 ± 0.002 Å |
α | 87.11 ± 0.03° |
β | 82.02 ± 0.03° |
γ | 88.24 ± 0.03° |
Cell volume | 994.5 ± 0.3 Å3 |
Cell temperature | 298 ± 2 K |
Ambient diffraction temperature | 298 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1855 |
Residual factor for significantly intense reflections | 0.0664 |
Weighted residual factors for significantly intense reflections | 0.1178 |
Weighted residual factors for all reflections included in the refinement | 0.1398 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.996 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7152223.html
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Users of the data should acknowledge the original authors of the
structural data.