Information card for entry 7152239

Structure parameters

• Formula: C24 H30 N2
• Calculated formula: C24 H30 N2
• Title of publication: One-pot preparation of piperazines by regioselective ring-opening of non-activated arylaziridines.
• Authors of publication: Trinchera, Piera; Musio, Biagia; Degennaro, Leonardo; Moliterni, Anna; Falcicchio, Aurelia; Luisi, Renzo
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2012
• Journal volume: 10
• Journal issue: 10
• Pages of publication: 1962 - 1965
• a: 8.4011 ± 0.0007 Å
• b: 10.0557 ± 0.0008 Å
• c: 13.0329 ± 0.0015 Å
• α: 74.541 ± 0.007°
• β: 78.907 ± 0.007°
• γ: 76.897 ± 0.006°
• Cell volume: 1023.28 ± 0.17 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1402
• Residual factor for significantly intense reflections: 0.0585
• Weighted residual factors for significantly intense reflections: 0.1212
• Weighted residual factors for all reflections included in the refinement: 0.1511
• Goodness-of-fit parameter for all reflections included in the refinement: 0.984
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No