Information card for entry 7152420
| Formula |
C47.5 H45 N O2 P2 |
| Calculated formula |
C47.5 H45 N O2 P2 |
| Title of publication |
Reactions of 1-alkyl-1,2-diphospholes with 1,3-dipoles: diphenyldiazomethane and nitrones. |
| Authors of publication |
Zagidullin, Almaz; Ganushevich, Yulia; Miluykov, Vasili; Krivolapov, Dmitry; Kataeva, Olga; Sinyashin, Oleg; Hey-Hawkins, Evamarie |
| Journal of publication |
Organic & biomolecular chemistry |
| Year of publication |
2012 |
| Journal volume |
10 |
| Journal issue |
27 |
| Pages of publication |
5298 - 5306 |
| a |
11.308 ± 0.0009 Å |
| b |
11.3298 ± 0.0009 Å |
| c |
15.5036 ± 0.0008 Å |
| α |
76.884 ± 0.003° |
| β |
88.093 ± 0.002° |
| γ |
85.182 ± 0.002° |
| Cell volume |
1927.4 ± 0.2 Å3 |
| Cell temperature |
150 ± 2 K |
| Ambient diffraction temperature |
150 ± 2 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0495 |
| Residual factor for significantly intense reflections |
0.0376 |
| Weighted residual factors for significantly intense reflections |
0.114 |
| Weighted residual factors for all reflections included in the refinement |
0.1211 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.18 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/7152420.html
