Information card for entry 7152724

Structure parameters

• Formula: C24 H20 N2 O3
• Calculated formula: C24 H20 N2 O3
• SMILES: O[C@]1(C(=O)N(Cc2ccccc2)c2c1cccc2)[C@@H]1c2ccccc2N(C1=O)C.O[C@@]1(C(=O)N(Cc2ccccc2)c2c1cccc2)[C@H]1c2ccccc2N(C1=O)C
• Title of publication: Rhodium(ii) catalyzed diastereoselective reactions of diazoacetamides with isatins: an efficient approach to 3-hydroxy-3,3'-bioxindoles.
• Authors of publication: Li, Ming; Zan, Li; Prajapati, Dipak; Hu, Wenhao
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2012
• Journal volume: 10
• Journal issue: 44
• Pages of publication: 8808 - 8813
• a: 24.8142 ± 0.001 Å
• b: 8.6804 ± 0.0003 Å
• c: 18.1721 ± 0.0007 Å
• α: 90°
• β: 99.492 ± 0.001°
• γ: 90°
• Cell volume: 3860.6 ± 0.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0708
• Residual factor for significantly intense reflections: 0.0421
• Weighted residual factors for significantly intense reflections: 0.0986
• Weighted residual factors for all reflections included in the refinement: 0.1172
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No