Information card for entry 7152974

Structure parameters

• Formula: C25 H23 N3 O
• Calculated formula: C25 H23 N3 O
• Title of publication: Aerobic C-H amination of tetrahydrocarbazole derivatives via photochemically generated hydroperoxides.
• Authors of publication: Gulzar, Naeem; Klussmann, Martin
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2013
• Journal volume: 11
• Journal issue: 27
• Pages of publication: 4516 - 4520
• a: 13.886 ± 0.0015 Å
• b: 9.6705 ± 0.001 Å
• c: 15.6885 ± 0.0016 Å
• α: 90°
• β: 99.869 ± 0.002°
• γ: 90°
• Cell volume: 2075.5 ± 0.4 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0659
• Residual factor for significantly intense reflections: 0.0462
• Weighted residual factors for significantly intense reflections: 0.1233
• Weighted residual factors for all reflections included in the refinement: 0.1384
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No