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Information card for entry 7153578
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Coordinates | 7153578.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C46 H46 N4 O5 |
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Calculated formula | C46 H46 N4 O5 |
Title of publication | Rhodium-catalyzed three-component reaction of 3-diazooxindoles with indoles and isatin-derived ketimines: a facile and versatile approach to functionalized 3,3',3''-trisindoles. |
Authors of publication | Mei, Liang-Yong; Tang, Xiang-Ying; Shi, Min |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2014 |
Journal volume | 12 |
Journal issue | 7 |
Pages of publication | 1149 - 1156 |
a | 8.9744 ± 0.0011 Å |
b | 18.096 ± 0.002 Å |
c | 24.959 ± 0.003 Å |
α | 97.516 ± 0.003° |
β | 99.857 ± 0.003° |
γ | 93.864 ± 0.002° |
Cell volume | 3942.5 ± 0.8 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1131 |
Residual factor for significantly intense reflections | 0.067 |
Weighted residual factors for significantly intense reflections | 0.1805 |
Weighted residual factors for all reflections included in the refinement | 0.212 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7153578.html
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Users of the data should acknowledge the original authors of the
structural data.