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Information card for entry 7153786
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Coordinates | 7153786.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | (R)-1-Benzyl-4-(methyl-tert-butylphosphino-borane)-1H-1,2,3-triazole |
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Formula | C14 H23 B N3 P |
Calculated formula | C14 H23 B N3 P |
Title of publication | Silyl alkynylphosphine-boranes: key precursors of triazolylphosphines via tandem desilylation-Click chemistry. |
Authors of publication | Veillard, Romain; Bernoud, Elise; Abdellah, Ibrahim; Lohier, Jean-François; Alayrac, Carole; Gaumont, Annie-Claude |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2014 |
Journal volume | 12 |
Journal issue | 22 |
Pages of publication | 3635 - 3640 |
a | 9.85 ± 0.0002 Å |
b | 11.141 ± 0.0002 Å |
c | 14.4209 ± 0.0003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1582.53 ± 0.05 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 5 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0396 |
Residual factor for significantly intense reflections | 0.0338 |
Weighted residual factors for significantly intense reflections | 0.0799 |
Weighted residual factors for all reflections included in the refinement | 0.0832 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.076 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7153786.html
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