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Information card for entry 7153877
Preview
Coordinates | 7153877.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C25 H24 |
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Calculated formula | C25 H24 |
SMILES | c1(cc2ccccc2cc1)/C=C/1[C@@H]2C[C@H]([C@@H]1c1ccc(cc1)C)CC2.c1(cc2ccccc2cc1)/C=C/1[C@H]2C[C@@H]([C@H]1c1ccc(cc1)C)CC2 |
Title of publication | Palladium-catalyzed three-component reaction of N-tosylhydrazone, norbornene and aryl halide. |
Authors of publication | Hu, Fangdong; Xia, Ying; Liu, Zhenxing; Ma, Chen; Zhang, Yan; Wang, Jianbo |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2014 |
Journal volume | 12 |
Journal issue | 22 |
Pages of publication | 3590 - 3593 |
a | 6.1765 ± 0.0002 Å |
b | 11.6169 ± 0.0004 Å |
c | 24.6124 ± 0.0011 Å |
α | 90° |
β | 96.136 ± 0.004° |
γ | 90° |
Cell volume | 1755.87 ± 0.11 Å3 |
Cell temperature | 100 ± 0.1 K |
Ambient diffraction temperature | 100 ± 0.1 K |
Number of distinct elements | 2 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0753 |
Residual factor for significantly intense reflections | 0.055 |
Weighted residual factors for significantly intense reflections | 0.1161 |
Weighted residual factors for all reflections included in the refinement | 0.1273 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.068 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7153877.html
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