Information card for entry 7154133

Structure parameters

• Formula: C32 H36 Cl N O
• Calculated formula: C32 H36 Cl N O
• Title of publication: Asymmetric synthesis of axially chiral anilides by Pd-catalyzed allylic substitutions with P/olefin ligands.
• Authors of publication: Liu, Yilin; Feng, Xiangqing; Du, Haifeng
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2015
• Journal volume: 13
• Journal issue: 1
• Pages of publication: 125 - 132
• a: 10.084 ± 0.002 Å
• b: 10.408 ± 0.002 Å
• c: 26.571 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2788.7 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0562
• Residual factor for significantly intense reflections: 0.0531
• Weighted residual factors for significantly intense reflections: 0.1128
• Weighted residual factors for all reflections included in the refinement: 0.1149
• Goodness-of-fit parameter for all reflections included in the refinement: 1.138
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No