Information card for entry 7154186

Structure parameters

• Chemical name: syn-5g
• Formula: C14 H14 N4 O4
• Calculated formula: C14 H14 N4 O4
• Title of publication: A facile approach to spirocyclic 2-azido indolines via azidation of indoles with ceric ammonium nitrate.
• Authors of publication: Li, Jing; Liu, Mao; Li, Qi; Tian, Hua; Shi, Yian
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2014
• Journal volume: 12
• Journal issue: 48
• Pages of publication: 9769 - 9772
• a: 7.764 ± 0.003 Å
• b: 9.345 ± 0.004 Å
• c: 20.472 ± 0.009 Å
• α: 80.083 ± 0.016°
• β: 86.694 ± 0.016°
• γ: 79.18 ± 0.013°
• Cell volume: 1436.6 ± 1 ų
• Cell temperature: 173.15 K
• Ambient diffraction temperature: 173.15 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1272
• Residual factor for significantly intense reflections: 0.1109
• Weighted residual factors for significantly intense reflections: 0.3066
• Weighted residual factors for all reflections included in the refinement: 0.3194
• Goodness-of-fit parameter for all reflections included in the refinement: 1.123
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No