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Information card for entry 7154362
Preview
Coordinates | 7154362.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H26 O5 S |
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Calculated formula | C24 H26 O5 S |
SMILES | S1(=O)(=O)[C@@H]2[C@](O)(C[C@H]([C@H]1C(=C2)C)c1ccc(OC)cc1)/C=C/c1ccc(OC)cc1.S1(=O)(=O)[C@H]2[C@@](O)(C[C@@H]([C@@H]1C(=C2)C)c1ccc(OC)cc1)/C=C/c1ccc(OC)cc1 |
Title of publication | Diastereoselective tandem reactions of substituted 3-sulfolenes with bis-vinyl ketones leading to highly functionalized bicyclic and tricyclic frameworks. |
Authors of publication | Brant, Michael G.; Friedmann, Jordan N.; Bohlken, Connor G.; Oliver, Allen G.; Wulff, Jeremy E. |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2015 |
Journal volume | 13 |
Journal issue | 15 |
Pages of publication | 4581 - 4588 |
a | 9.7206 ± 0.0004 Å |
b | 14.2444 ± 0.0005 Å |
c | 15.3744 ± 0.0005 Å |
α | 95.035 ± 0.0014° |
β | 95.523 ± 0.0015° |
γ | 96.46 ± 0.0015° |
Cell volume | 2094.98 ± 0.13 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0609 |
Residual factor for significantly intense reflections | 0.0402 |
Weighted residual factors for significantly intense reflections | 0.091 |
Weighted residual factors for all reflections included in the refinement | 0.1013 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.014 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7154362.html
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Users of the data should acknowledge the original authors of the
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