Copper(ii) catalyzed synthesis of novel helical luminescent benzo[4,5]imidazo[1,2-a][1,10]phenanthrolines via an intramolecular C-H amination reaction.
Authors of publication
Borges da Silva, Ramon; Teixeira, Rodolfo Inêz; Wardell, James L.; Wardell, Solange M. S. V.; Garden, Simon J.
Journal of publication
Organic & biomolecular chemistry
Year of publication
2017
Journal volume
15
Journal issue
4
Pages of publication
812 - 826
a
15.7235 ± 0.0004 Å
b
7.2386 ± 0.0002 Å
c
25.4616 ± 0.0007 Å
α
90°
β
96.401 ± 0.003°
γ
90°
Cell volume
2879.87 ± 0.14 Å3
Cell temperature
100.01 ± 0.1 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0738
Residual factor for significantly intense reflections
0.0532
Weighted residual factors for significantly intense reflections
0.1128
Weighted residual factors for all reflections included in the refinement
0.1223
Goodness-of-fit parameter for all reflections included in the refinement
