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Information card for entry 7156172
Preview
Coordinates | 7156172.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C14 H16 Cl N3 O6 S |
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Calculated formula | C14 H16 Cl N3 O6 S |
Title of publication | An asymmetric Mannich reaction of α-diazocarbonyl compounds and N-sulfonyl cyclic ketimines catalyzed by complexes generated from chiral and achiral phosphines with gold(i). |
Authors of publication | Zhou, Minghui; Su, Qin; Addepalli, Yesu; He, Yun; Wang, Zhen |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2018 |
Journal volume | 16 |
Journal issue | 16 |
Pages of publication | 2923 - 2931 |
a | 7.8621 ± 0.0004 Å |
b | 10.129 ± 0.0005 Å |
c | 12.5926 ± 0.0005 Å |
α | 70.829 ± 0.004° |
β | 76.104 ± 0.004° |
γ | 67.503 ± 0.005° |
Cell volume | 867.55 ± 0.08 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293.15 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0752 |
Residual factor for significantly intense reflections | 0.0492 |
Weighted residual factors for significantly intense reflections | 0.1246 |
Weighted residual factors for all reflections included in the refinement | 0.1343 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.098 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7156172.html
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