Studies on the interactions of 5-R-3-(2-pyridyl)-1,2,4-triazines with arynes: inverse demand aza-Diels-Alder reaction versus aryne-mediated domino process.
Authors of publication
Kopchuk, Dmitry S.; Nikonov, Igor L.; Khasanov, Albert F.; Giri, Kousik; Santra, Sougata; Kovalev, Igor S.; Nosova, Emiliya V.; Gundala, Sravya; Venkatapuram, Padmavathi; Zyryanov, Grigory V.; Majee, Adinath; Chupakhin, Oleg N.
Journal of publication
Organic & biomolecular chemistry
Year of publication
2018
Journal volume
16
Journal issue
28
Pages of publication
5119 - 5135
a
9.2421 ± 0.0005 Å
b
17.3468 ± 0.0011 Å
c
28.1793 ± 0.0014 Å
α
90°
β
90°
γ
90°
Cell volume
4517.7 ± 0.4 Å3
Cell temperature
295 K
Ambient diffraction temperature
294 K
Number of distinct elements
4
Space group number
61
Hermann-Mauguin space group symbol
P b c a
Hall space group symbol
-P 2ac 2ab
Residual factor for all reflections
0.2187
Residual factor for significantly intense reflections
0.0624
Weighted residual factors for significantly intense reflections
0.1014
Weighted residual factors for all reflections included in the refinement
0.152
Goodness-of-fit parameter for all reflections included in the refinement
