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Information card for entry 7156285
Preview
Coordinates | 7156285.cif |
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Original paper (by DOI) | HTML |
Formula | C19 H16 Br N3 O5 S |
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Calculated formula | C19 H16 Br N3 O5 S |
Title of publication | Diastereo- and enantioselective Mannich/cyclization cascade reaction of isocyanoacetates with cyclic sulfamide ketimines by cinchona alkaloid squaramide/AgOAc cooperative catalysis. |
Authors of publication | Zhao, Mei-Xin; Dong, Zhi-Wen; Zhu, Guang-Yu; Zhao, Xiao-Li; Shi, Min |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2018 |
Journal volume | 16 |
Journal issue | 25 |
Pages of publication | 4641 - 4649 |
a | 7.3579 ± 0.0003 Å |
b | 8.8158 ± 0.0004 Å |
c | 15.8511 ± 0.0007 Å |
α | 85.431 ± 0.001° |
β | 88.543 ± 0.001° |
γ | 72.739 ± 0.001° |
Cell volume | 978.77 ± 0.07 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0397 |
Residual factor for significantly intense reflections | 0.0342 |
Weighted residual factors for significantly intense reflections | 0.0907 |
Weighted residual factors for all reflections included in the refinement | 0.0941 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.057 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7156285.html
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