Crystallography Open Database

Information card for entry 7156291

Preview

Structure parameters

Formula	C21 H28 N2 O2
Calculated formula	C21 H28 N2 O2
Title of publication	Auto-oxidation promoted sp<sup>3</sup> C-H arylation of glycine derivatives.
Authors of publication	Wei, Yuanyuan; Wang, Jie; Wang, Yajun; Yao, Xiaoqiang; Yang, Caixia; Huo, Congde
Journal of publication	Organic & biomolecular chemistry
Year of publication	2018
Journal volume	16
Journal issue	27
Pages of publication	4985 - 4989
a	23.0931 ± 0.0006 Å
b	6.0038 ± 0.0002 Å
c	29.114 ± 0.0007 Å
α	90°
β	99.674 ± 0.001°
γ	90°
Cell volume	3979.15 ± 0.19 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0737
Residual factor for significantly intense reflections	0.0552
Weighted residual factors for significantly intense reflections	0.1524
Weighted residual factors for all reflections included in the refinement	0.1624
Goodness-of-fit parameter for all reflections included in the refinement	0.986
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7156291.html