Information card for entry 7156297

Structure parameters

• Formula: C19 H18 Cl N O3 S
• Calculated formula: C19 H18 Cl N O3 S
• Title of publication: Silver(i)-catalyzed sequential hydroamination and Prins type cyclization for the synthesis of fused benzo-δ-sultams.
• Authors of publication: Maheshwar Rao, B.; Yadav, J. S.; Sridhar, B.; Subba Reddy, B. V.
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2018
• Journal volume: 16
• Journal issue: 28
• Pages of publication: 5163 - 5166
• a: 15.5285 ± 0.0011 Å
• b: 12.2909 ± 0.0009 Å
• c: 18.3647 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3505.1 ± 0.4 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0649
• Residual factor for significantly intense reflections: 0.0575
• Weighted residual factors for significantly intense reflections: 0.1637
• Weighted residual factors for all reflections included in the refinement: 0.1716
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No