Information card for entry 7156372

Structure parameters

• Common name: (R)-6, 6?-HMSIOL
• Formula: C29 H42 O3
• Calculated formula: C29 H42 O3
• Title of publication: Synthesis and application of a new chiral monodentate spiro phosphoramidite ligand based on hexamethyl-1,1'-spirobiindane backbone in asymmetric hydroamination/arylation of alkenes.
• Authors of publication: Shan, Huanyu; Pan, Rihuang; Lin, Xufeng
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2018
• Journal volume: 16
• Journal issue: 34
• Pages of publication: 6183 - 6186
• a: 10.811 ± 0.0004 Å
• b: 11.3987 ± 0.0003 Å
• c: 11.7982 ± 0.0004 Å
• α: 90°
• β: 104.616 ± 0.004°
• γ: 90°
• Cell volume: 1406.86 ± 0.08 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293.15 K
• Number of distinct elements: 3
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0563
• Residual factor for significantly intense reflections: 0.0466
• Weighted residual factors for significantly intense reflections: 0.124
• Weighted residual factors for all reflections included in the refinement: 0.1356
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No