Crystallography Open Database

Information card for entry 7156389

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Structure parameters

Formula	C26 H20 Cl N3 O8 S
Calculated formula	C26 H20 Cl N3 O8 S
Title of publication	Synthesis of polycyclic spirooxindoles via an asymmetric catalytic one-pot stepwise Aldol/chloroetherification/aromatization procedure.
Authors of publication	Jiang, Yan; Yu, Shuo-Wen; Yang, Yi; Liu, Ying-Le; Xu, Xiao-Ying; Zhang, Xiao-Mei; Yuan, Wei-Cheng
Journal of publication	Organic & biomolecular chemistry
Year of publication	2018
Journal volume	16
Journal issue	36
Pages of publication	6647 - 6651
a	5.6165 ± 0.0018 Å
b	13.983 ± 0.002 Å
c	16.7686 ± 0.0017 Å
α	65.52 ± 0.03°
β	88.6 ± 0.03°
γ	86.77 ± 0.03°
Cell volume	1196.6 ± 0.5 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2192
Residual factor for significantly intense reflections	0.0706
Weighted residual factors for significantly intense reflections	0.101
Weighted residual factors for all reflections included in the refinement	0.1237
Goodness-of-fit parameter for all reflections included in the refinement	0.898
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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