Information card for entry 7156425

Structure parameters

• Formula: C24 H28 N4 O Si
• Calculated formula: C24 H28 N4 O Si
• Title of publication: Efficient synthesis of tetrazole hemiaminal silyl ethers via three-component hemiaminal silylation.
• Authors of publication: Xie, Ming-Sheng; Cheng, Xuan; Chen, Yang-Guang; Wu, Xiao-Xia; Qu, Gui-Rong; Guo, Hai-Ming
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2018
• Journal volume: 16
• Journal issue: 38
• Pages of publication: 6890 - 6894
• a: 11.4816 ± 0.0008 Å
• b: 12.2451 ± 0.0006 Å
• c: 16.6439 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2340 ± 0.2 ų
• Cell temperature: 292.64 ± 0.1 K
• Ambient diffraction temperature: 292.64 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0538
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.085
• Weighted residual factors for all reflections included in the refinement: 0.0911
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No