Information card for entry 7156439
| Formula |
C25 H24 O5 |
| Calculated formula |
C25 H24 O5 |
| Title of publication |
Atom-economic synthesis of cyclobuta[a]naphthalen-4-ols via a base-promoted [2 + 2] cycloaddition/1,6-nucleophilic addition cascade. |
| Authors of publication |
Wang, Jia-Yin; Xie, Feng-Lie; Hu, Jian-Qiang; Yang, Shi-Zhao; Wang, You-Jian; Hao, Wen-Juan; Tu, Shu-Jiang; Jiang, Bo |
| Journal of publication |
Organic & biomolecular chemistry |
| Year of publication |
2018 |
| Journal volume |
16 |
| Journal issue |
39 |
| Pages of publication |
7104 - 7108 |
| a |
9.4624 ± 0.0008 Å |
| b |
10.6408 ± 0.0009 Å |
| c |
12.1773 ± 0.0011 Å |
| α |
65.565 ± 0.001° |
| β |
86.673 ± 0.002° |
| γ |
68.952 ± 0.001° |
| Cell volume |
1035.87 ± 0.16 Å3 |
| Cell temperature |
298 ± 2 K |
| Ambient diffraction temperature |
298 ± 2 K |
| Number of distinct elements |
3 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0755 |
| Residual factor for significantly intense reflections |
0.0471 |
| Weighted residual factors for significantly intense reflections |
0.1048 |
| Weighted residual factors for all reflections included in the refinement |
0.1151 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.049 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7156439.html
