Information card for entry 7156441

Structure parameters

• Formula: C44 H66 O8 P2 Rh2
• Calculated formula: C44 H66 O8 P2 Rh2
• Title of publication: Dirhodium(ii)/P(t-Bu)₃ catalyzed tandem reaction of α,β-unsaturated aldehydes with arylboronic acids.
• Authors of publication: Ma, Ziling; Wang, Yuanhua
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2018
• Journal volume: 16
• Journal issue: 40
• Pages of publication: 7470 - 7476
• a: 8.9977 ± 0.0004 Å
• b: 10.0861 ± 0.0006 Å
• c: 14.7007 ± 0.0006 Å
• α: 86.402 ± 0.004°
• β: 72.916 ± 0.004°
• γ: 65.81 ± 0.005°
• Cell volume: 1160.73 ± 0.11 ų
• Cell temperature: 294.24 ± 0.1 K
• Ambient diffraction temperature: 294.24 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0466
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.1138
• Weighted residual factors for all reflections included in the refinement: 0.12
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No