Information card for entry 7156541

Structure parameters

• Formula: C24 H19 N O3
• Calculated formula: C24 H19 N O3
• Title of publication: Oxidative cross-dehydrogenative [2 + 3] annulation of α-amino ketones with α-keto esters: concise synthesis of clausenamide analogues.
• Authors of publication: Bhajammanavar, Vinod; Mallik, Sumitava; Baidya, Mahiuddin
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2019
• Journal volume: 17
• Journal issue: 7
• Pages of publication: 1740 - 1743
• a: 5.8336 ± 0.0006 Å
• b: 11.4947 ± 0.0015 Å
• c: 14.982 ± 0.002 Å
• α: 77.575 ± 0.005°
• β: 81.412 ± 0.005°
• γ: 77.375 ± 0.004°
• Cell volume: 951.8 ± 0.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.085
• Residual factor for significantly intense reflections: 0.0512
• Weighted residual factors for significantly intense reflections: 0.1273
• Weighted residual factors for all reflections included in the refinement: 0.151
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No