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Information card for entry 7156658
Preview
Coordinates | 7156658.cif |
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Original paper (by DOI) | HTML |
Chemical name | N-(trans-2-Iodocyclohexyl)-N-(phenylsulfonyl)benzenesulfonamide |
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Formula | C18 H20 I N O4 S2 |
Calculated formula | C18 H20 I N O4 S2 |
Title of publication | Efficient metal-free aminoiodination of alkenes with N-fluorobenzenesulfonimide under mild conditions. |
Authors of publication | Lei, Bowen; Miao, Qi; Ma, Lifang; Fu, Ruoqi; Hu, Fangrong; Ni, Ni; Li, Ziyuan |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2019 |
Journal volume | 17 |
Journal issue | 8 |
Pages of publication | 2126 - 2133 |
a | 10.9656 ± 0.0008 Å |
b | 14.167 ± 0.0012 Å |
c | 14.562 ± 0.003 Å |
α | 112.022 ± 0.014° |
β | 102.093 ± 0.011° |
γ | 104.464 ± 0.007° |
Cell volume | 1911.4 ± 0.5 Å3 |
Cell temperature | 108 ± 1 K |
Ambient diffraction temperature | 108 ± 1 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0397 |
Residual factor for significantly intense reflections | 0.0329 |
Weighted residual factors for significantly intense reflections | 0.0723 |
Weighted residual factors for all reflections included in the refinement | 0.0766 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7156658.html
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