Information card for entry 7156660

Structure parameters

• Formula: C17 H22 N2 O2
• Calculated formula: C17 H22 N2 O2
• Title of publication: HFIP-promoted Michael reactions: direct para-selective C-H activation of anilines with maleimides.
• Authors of publication: Li, Bang; Mao, Qi; Zhou, Jia; Liu, Feng; Ye, Na
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2019
• Journal volume: 17
• Journal issue: 8
• Pages of publication: 2242 - 2246
• a: 18.8452 ± 0.0014 Å
• b: 5.9542 ± 0.0004 Å
• c: 27.679 ± 0.002 Å
• α: 90°
• β: 103.868 ± 0.002°
• γ: 90°
• Cell volume: 3015.3 ± 0.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0632
• Residual factor for significantly intense reflections: 0.0522
• Weighted residual factors for significantly intense reflections: 0.1608
• Weighted residual factors for all reflections included in the refinement: 0.1714
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No